Synlett

Electrosynthesis of fluorinated benzo [b] thiophene derivatives

B Yin, S Inagi, T Fuchigami

Index: Yin, Bin; Inagi, Shinsuke; Fuchigami, Toshio Synlett, 2011 , # 9 p. 1313 - 1317

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Abstract

Abstract Anodic fluorination of benzo [b] thiophene derivatives provided a complex mixture of di-and trifluorinated products. On the other hand, anodic fluorination of 3-oxo-2, 3- dihydrobenzo [b] thiophene and methyl 3-oxo-2, 3-dihydrobenzo [b] thiophene-2- carboxylate gave the corresponding monofluorinated products selectively in moderate yields. Anodic fluorination of methyl α-(2-cyanophenylthio) acetate followed by ...

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