On the synthesis of α-amino sulfoxides
PJ Rayner, G Gelardi, P O'Brien, RAJ Horan…
Index: Organic and Biomolecular Chemistry, , vol. 12, # 21 p. 3499 - 3512
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Abstract
... sulfide 4 was synthesised by Beak-style α-lithiation-trapping of the parent N-Boc piperidine and sulfide 5 was accessed via iminium ion chemistry. ... Scheme 12, ... The organic layer was washed with 10% Na 2 S 2 O 3(aq) (50 mL), dried (Na 2 SO 4 ) and evaporated under reduced ...
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