Anchored Pd-complexes in mesoporous supports: Synthesis, characterization and catalysis studies for carbonylation reactions
BR Sarkar, RV Chaudhari
Index: Sarkar, Bibhas R.; Chaudhari, Raghunath V. Catalysis Today, 2012 , vol. 198, # 1 p. 154 - 173
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Citation Number: 6
Abstract
Pd (pyca)(PPh3)(OTs)[pyca= 2-picolinate] complex is efficiently anchored inside different mesoporous matrices, such as MCM-41, MCM-48, SBA-15 using a molecular aminopropyl tether moiety employing different synthesis strategies. Thorough characterization of the materials using powder XRD, multinuclear (13C, 29Si, 31P) CP-MAS NMR, XPS, SEM, N2- sorption studies etc. confirmed the successful anchoring of the palladium complex to the ...
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