Journal of the American Chemical Society

Grignard Preparation of Fluorene-2-Carboxylic Acid1

DC Morrison

Index: Morrison Journal of the American Chemical Society, 1952 , vol. 74, p. 3431

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Citation Number: 2

Abstract

Experimental All m. ps. are corrected. Microanalyses by I r. R. Pyke. cE, Il-Ethoxy-2- chlorocyclohexanol-3~~ J~(A).-Instead of using chlorine gas, aqueous hypochlorous acid was prepared by acidifying commercial 5 or 12% sodium hypochlorite solution (available at grocery stores). About 0.09 mole of the hypochlorous acid solution was added at 0" in portions to 0.055 mole of l-ethoxycyclohexene-2.~ 2 After the last portion was added the ...