Further study of tris (cyclohexyl) stannane compounds, Cy 3 SnX. Syntheses of the compounds with X= Br, I, N 3 and NCS and redetermination of the crystal structures …

RA Howie, MVH Moura, JL Wardell, SMSV Wardell

Index: Howie, R. Alan; Moura, Marcelo V.H.; Wardell, James L.; Wardell, Solange M.S.V. Polyhedron, 2004 , vol. 23, # 14 p. 2331 - 2336

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Citation Number: 3

Abstract

Methods of preparation and far IR data are presented for various Cy3SnX compounds. The synthesis of tris (cyclohexyl) tin hydroxide, Cy3SnOH, is also described. Redeterminations of the crystal structures of tris (cyclohexyl) tin bromide and iodide, Cy3SnBr and Cy3SnI, confirm their molecular nature and improve considerably upon the results reported earlier [S. Calogero, P. Ganis, V. Peruzzo, G. Tagliavini, G. Valle, J. Organomet. Chem. 220 (1981) ...