Piperidine Derivatives. XXIII. Certain Halogenated 1-Methyl-4-Phenylpiperidines and Related Compounds

SM McElvain, JC Safranski Jr

Index: McElvain; Safranski Journal of the American Chemical Society, 1950 , vol. 72, p. 3134,3135

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Citation Number: 18

Abstract

Summary The preparation and nitration of 2-imidazoli- done, ethylenebisurethan, ethylenebisacetamide and cyclic eihyleneoxamide to dinitro derivatives and the hydrolysis of the dinitro derivatives to the high explosive ethylenedinitramine (EDNA) are described. Ethylenebisurea, which was prepared from ethylenediamine and urea, is nitrated at the terminal amino groups. In two instances a mixture of acetic anhydride and 98% nitric acid was able to nitrate com- pounds which ...

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