A Facile Synthesis of 4, 6-Dimethoxy-2-methylsulfonylpyrimidine
D Xu, Z Zhu, H Xu, Z Wang
Index: Xu, Defeng; Zhu, Zhiling; Xu, Hui; Wang, Ziqiao Asian Journal of Chemistry, 2014 , vol. 26, # 1 p. 313 - 314
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Abstract
Abstract A facile and efficient synthesis of 4, 6-dimethoxy-2-methylthiopyrimidine can be achieved by nucleophilic substitution of 2-chloro-4, 6-dimethoxypyrimidine with sodium methyl mercaptide for a 95.6% yield. 4, 6-Dimethoxy-2-methylsulfonylpyrimidine can be produced via oxidation using hydrogen peroxide in the presence of sodium tungstate dihydrate in a 95% yield.[PUBLICATION ABSTRACT]
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