The Journal of Organic Chemistry

Synthesis of halogenated phosphonoacetate esters

CE McKenna, LA Khawli

Index: McKenna, Charles E.; Khawli, Leslie A. Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5467 - 5471

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Citation Number: 49

Abstract

24.9 (4,'JcH= 134, CH, CBr) 50.7 (d,'JcP= 150, CH, CBr) 62.7 (t,'JCH= 148, CHz [CO]) 64.4 (t,'JCH= 149,'Jcp= 7, 2 CHz [PO] 167.5 (s, C= O) analogous fluorination of tetraalkyl methanedipho~ phonates.~ However, examination of the literature reveals that several of the remaining possible halogenated PA4 esters have never been described, while for others the available synthetic procedures are not fully satisfactory. We report here detailed ...