The solution thermolysis of 2-, 3-, and 4-(2-hydroxy-2-arylethyl) pyridines
Y Houminer, DL Williams
Index: Houminer, Yoram; Williams, David L. Journal of Organic Chemistry, 1983 , vol. 48, # 15 p. 2622 - 2625
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Citation Number: 5
Abstract
0022-3263/83/1948-2622 $01.50/0 compounds gave satisfactory spectral and physical data. Benzene was distilled in a Nz atmosphere from benzophenone ketyl and then was stirred over the disodium salt of EDTA. Dioxaphosphoranes 3 and 4. These compounds were synthesized by addition of phosphine 2 via syringe to a serum capped 10-mm NMR tube containing 1 and benzene at-78 “C. The reaction mixture was then allowed to warm to ...
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