Organic Process Research & Development

… Ethyl-Substituted Silanes from Ethylchloride, Tetraethoxysilane, and Organotrichlorosilane for Production of Polyethylsiloxane Liquids. 1. Batch One-Step Synthesis of …

BA Klokov

Index: Klokov, Boris A. Organic Process Research and Development, 2000 , vol. 4, # 1 p. 49 - 54

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Citation Number: 2

Abstract

Development of batch one-step manufacturing process for ethylethoxy-and ethylchlorosilanes is desribed. The methodology of synthesis of ethyl-substituted silanes has been improved. The important factors for the successful synthesis have been determined. Among them are the replacement of the part tetraethoxysilane 3 by ethyltrichlorosilane 10, the optimum concentration of 3 and 10 resulting in high yield of triethylsilanes, low ...