Characterization and Comparative Studies on Conventional and Microwave Synthesis of Some Disulfides

NT Karakullukcu, H Yakan, S Ozturk…

Index: Karakullukcu, Nalan Turkoz; Yakan, Hasan; Ozturk, Seyhan; Kutuk, Halil Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 11 p. 1576 - 1583

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Abstract

Some disulfide derivatives have been prepared by microwave assisted synthesis methodology from thiophthalimides(sulfenimides) and thiols in a modified microwave oven under reflux at 600 Watt in ethanol. Elucidation of the structures of the synthesized compounds has been performed by IR, 1 H NMR, and 13 C NMR spectroscopic methods. ... Some disulfide derivatives have been prepared by microwave assisted synthesis methodology from ...