The Journal of Organic Chemistry

The alkylation of benzene with 1, 2-dichloroalkanes

DL Ransley

Index: Ransley,D.L. Journal of Organic Chemistry, 1966 , vol. 31, p. 3595 - 3599

Full Text: HTML

Citation Number: 7

Abstract

We were not able, on our Carbowax column, to separate all the isomers of diphenylbutane which constituted 14.3% of the product. Compound 16 was obtained pure by preparative vpc and the meso isomer of 18 was obtained crystalline (mp 125'). The nmr of 15 and 17 were both distinctive and the mass spectral cracking patterns of the mixture showed the gross features to be expected. There was also some spectral evidence for the 1, 2 isomer, but ...

 Related Synthetic Route
(4-chloro-1,1-dimethyl-butyl)-benzene Structure

1985-95-1

(4-chloro-1,1-d...

~%

1,1-Dimethyltetralin Structure

1985-59-7

1,1-Dimethyltetralin

1.2-Dichlor-4-methyl-pentan Structure

13556-76-8

1.2-Dichlor-4-m...

~%

1,1-Dimethyltetralin Structure

1985-59-7

1,1-Dimethyltetralin

benzene Structure

71-43-2

benzene

~%

1,1-Dimethyltetralin Structure

1985-59-7

1,1-Dimethyltetralin

N/A Structure

26198-63-0

N/A

benzene Structure

71-43-2

benzene

~%

Cumene Structure

98-82-8

Cumene

Benzene,1,1'-(1-methyl-1,2-ethanediyl)bis- Structure

5814-85-7

Benzene,1,1'-(1...

Detail
Butane, 1,2-dichloro- Structure

616-21-7

Butane, 1,2-dic...

benzene Structure

71-43-2

benzene

~%

1-phenylbutylbenzene Structure

719-79-9

1-phenylbutylbenzene

1-methyl-3-phenylindan Structure

6416-39-3

1-methyl-3-phen...

Butane, 1,2-dichloro- Structure

616-21-7

Butane, 1,2-dic...

benzene Structure

71-43-2

benzene

~%

1-phenylbutylbenzene Structure

719-79-9

1-phenylbutylbenzene

(1-Methylpropane-1,3-Diyl)Dibenzene Structure

1520-44-1

(1-Methylpropan...

Detail
Butane, 1,2-dichloro- Structure

616-21-7

Butane, 1,2-dic...

benzene Structure

71-43-2

benzene

~%

1-phenylbutylbenzene Structure

719-79-9

1-phenylbutylbenzene

(1-Methylpropane-1,3-Diyl)Dibenzene Structure

1520-44-1

(1-Methylpropan...

Detail
benzene Structure

71-43-2

benzene

~%

4-methylpentylbenzene Structure

4215-86-5

4-methylpentylb...

1,1-Dimethyltetralin Structure

1985-59-7

1,1-Dimethyltetralin

~%

4-methylpentylbenzene Structure

4215-86-5

4-methylpentylb...

(4-chloro-1,1-dimethyl-butyl)-benzene Structure

1985-95-1

(4-chloro-1,1-d...

~%

4-methylpentylbenzene Structure

4215-86-5

4-methylpentylb...


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