By Lithium Aluminum Hydride.-To a solution of 88 mg. of Reduction of the Diester (I) to the Glycol (IV). lifhium aluminum hydride in 18 cc. of anhydrous ether ... (prepared as described above) was added in small portion> a solution of 0.45 g. of the dimethyl ester of cis-2-methyl- 2-carboxycyclohexaneacetic acid (I, prepared by esterifi - cation of the acid4) at room temperature over a period of fifteen minutes; a colorless gelatinous precipitate ap- peared immediately. After standing at room ...
