The Journal of Organic Chemistry

Notes: The Structure of 2-Substituted Amino-1, 3, 4-thiadiazoles

B Stanovnik, M Tisler

Index: Stanovnik,B.; Tisler,M. Journal of Organic Chemistry, 1960 , vol. 25, p. 2234 - 2236

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Citation Number: 20

Abstract

4-Methy1-4-phenylthiosemicarbazide. This compound was prepared from carboxymethyl N- methyl-N-phenyl dithiocarbamate12 (8.8 g.), which was heated on a water bath with excess hydrazine hydrate (15 ml. of SOOj,) for 10 min. After cooling to roam temperature the mixture wa8 diluted with an equal volume of water and the precipitate collected.