Ketene Acetals. V. The Reaction of Ketene Diethylacetal with Various Compounds Containing an Active Hydrogen1

…, D Kundiger, SM McElvain

Index: Barnes; Kundiger; McElvain Journal of the American Chemical Society, 1940 , vol. 62, p. 1285

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Citation Number: 8

Abstract

Discussion That reduction of the dichloronitrobenzenes occurs in definite stages is clearly borne out by some of the experiments. The one involving the action of diethanolamine on 3, k-dichloronitrobenzene is representative. When the two are refluxed together for a period of two hours, the only reduction product isolated is the azo compound; if heating is continued for four hours, no tetrachloroazobenzene can be identified, but reduction to the amino ...