4978 J. Org. Chem., Vol. 43, No. 26, 1978 Moore and Driscoll groine (bp 60-100" C) to give 88.4 g of amine: mp 75.5-79.5" C. Mass spectrum, m/e (relative intensity): 328 (< 1), which corresponds to the molecular ion for 9; 283 (7) and 281 (5), which correspond to the molecular ion for 8; 241 (12), 239 (671, and 237 (loo), which correspond to the molecular ion for 10. Anal. Calcd for 62.9% 10, 28.6% 8, and 8.5% 9: C, 58.24; H, 3.69; Br, 8.09; C1, ...
