Reactions of 2, 2, 6, 6-tetrachlorohexanone with substituted anilines and ammonia. Synthesis of 5-nitro and 5-amino analogs of orthophen

IP Graevskaya, VA Azimov, SY Ryabova…

Index: Graevskaya; Azimov; Ryabova; Alekseeva; Anisimova; Syubaev; Granik Pharmaceutical Chemistry Journal, 1998 , vol. 32, # 1 p. 41 - 44

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Abstract

... SYNTHESIS OF 5-NITRO AND 5-AMINO ANALOGS OF ORTHOPHEN IP Graevskaya, ~ VA Azimov, t S. Yu. Ryabova, t LM Alekseeva, I OS Anisimova, I RD Syubaev, t and VG Granik 1 Translated from Khimiko-Farmatsevticheskii Zhurnal, Vol. 32, No. 1, pp. ... Page 4. 44 !. P. Graevskaya et al. added 5 ml of 2-propanol, and the stirring continued for ! h at 95 - 100~ Then the mixture was cooled and diluted with 50 ml toluene and 10 ml methanol. ...