... Volume: Page: ... LiAlH 4 /AlCl 3 or hydrogenation of 7 over Raney nickel in the presence of NH 3 /EtOH gave crude (8-methoxy-10 ... Briefly, reaction of phthalic anhydride with the Grignard reagent from p-bromoanisole gave the 2-benzoylbenzoic acid derivative 10b ...