Abstract A new series of hydrazinecarboxamides (5a–n), bearing various methoxyphenyl and methoxyphenethyl groups, was synthesized by condensation of corresponding acid hydrazides (3a–f) with methoxyphenylisocyanates (4a–c). Dehydrocyclization of hydrazinecarboxamides (5a–n) yielded corresponding methoxyphenyl and methoxyphenethyl substituted triazoles (6a–l) by refluxing in 2 N aqueous sodium ...