Total synthesis of the racemic alkaloid diptocarpamine

OV Tolstikova, AG Tolstikov, VS Shmakov…

Index: Tolstikova, O. V.; Tolstikov, A. G.; Shmakov, V. S.; Galkin, E. G.; Vyrypaev, E. M.; et al. Chemistry of Natural Compounds, 1989 , vol. 25, p. 199 - 202 Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 232 - 236

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Abstract

V l is the volume of the total acetone extract, ml; ... V 2 is the volume of extract deposited on the plate, ml; ... P is the weight of the raw material, g; and h is the loss in weight on the drying of raw material, %. ... A procedure has been developed for the selective quantitative determination of the triterpene saponins in hawthorn fruit (haws) with the aid of chromato-photodensitometry. The relative error does not exceed ±5.1%.