Tetrahedron

Pheromone synthesis. Part 243: Synthesis and biological evaluation of (3R, 13R, 1′ S)-1′-ethyl-2′-methylpropyl 3, 13-dimethylpentadecanoate, the major …

K Mori, T Tashiro, B Zhao, DM Suckling, AM El-Sayed

Index: Tetrahedron, , vol. 66, # 14 p. 2642 - 2653

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Abstract

... Tetrahedron. Volume 66, Issue 14, 3 April 2010, Pages 2642–2653. ... Reagents: (a) LiAlH 4 , Et 2 O; (b) TsCl, C 5 H 5 N (51% for 7); (c) LiBr, DMF [78% based on (R)-2, three steps]; (d) (i) (R)-5, Mg, THF; (ii) 7, THF, Li 2 CuCl 4 [42% based on (R)-5 or 66% based on 7]; (e) Ac 2 O ...