The Journal of Organic Chemistry

Preparation of [1-(arylimino) alkyl] zinc by the. alpha.-addition of organozinc to isocyanide

M Murakami, H Ito, Y Ito

Index: Murakami, Masahiro; Ito, Hirohide; Ito, Yoshihiko Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4158 - 4159

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Citation Number: 24

Abstract

The heteronuclear HOHAHA technique was instru- mental in assigning carbons in rings E and G and other carbons that were problematic due to ring flexibility as well as severe overlapping in the proton region. Although the experiment described here is by no means an alternative to the more sensitive experiments like heteronuclear multiple quantum coherence (HMQC),16 it clearly provides an improvement in sensitivity and resolution over other currently ...