A solution of 300 g.(3.3 moles) of methallyl chloride in 300 g.(3.8 moles) of benzene was added during two hours to a well-stiired mixture of 500 g.(6.4 Omoles) of benzene and 400 g. of 96% sulfuric acid at 0-5. After an additional one-half hour of stirring, the upper layer was separated from the 433 g. of lower layer, washed with water, dried, and distilled under reduced pressure. Neophy! chloride (ie,(8-chloro-t-butyl)-benzene) boiling at 90-91 at 9 ...
