The Journal of organic chemistry

Design of polyaromatic hydrocarbon-supported tin reagents: A new family of tin reagents easily removable from reaction mixtures

D Stien, S Gastaldi

Index: Blanton, James R.; Salley, Joseph M. Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 490 - 491

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Citation Number: 32

Abstract

... Journal of ... J. Org. ... a Reagents and conditions: (a) tetrabutylammonium hydroxide, dioxane; R-Br, dioxane, 95 °C (1a, 80%; 1b, 62%); (b) NaI (15 equiv), acetone, 50 °C, 12 h (98%, 1c/1b = 9/1); (c) Bu 2 SnHCl, AIBN, CH 2 Cl 2 ; (d) Bu 2 SnHPh, Pd(OH) 2 /C; (e) Bu 2 SnHLi, THF. ...