Very rapid preparation of SmI2 by sonic treatment of iodoform and metallic samarium

JM Concellón, H Rodríguez??Solla…

Index: Concellon, Jose M.; Rodriguez-Solla, Humberto; Bardales, Eva; Huerta, Monica European Journal of Organic Chemistry, 2003 , # 9 p. 1775 - 1778

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Citation Number: 4

Abstract

Abstract A very rapid preparation of SmI 2 by sonication of a mixture of metallic samarium and iodoform in THF is described. To prove the synthetic applications of the obtained SmI 2 several high-yielding reactions were carried out. Preliminary results for the generation of SmI 2 in THF by sonication from diiodomethane, 1, 2-diiodoethane, or iodine are also described.(© Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)