New Preparation of 1, 2, 4, 5-Tetraoxanes

AO Terent'ev, AV Kutkin, ZA Starikova, MY Antipin…

Index: Terent'ev; Kutkin; Starikova; Antipin; Ogibin; Nikishin Synthesis, 2004 , # 14 p. 2356 - 2366

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Citation Number: 47

Abstract

Abstract A convenient procedure was developed for the synthesis of 1, 2, 4, 5-tetraoxanes based on the reaction of gem-bishydroperoxycycloalkanes with ketals and acetals catalyzed by boron trifluoride etherate, which makes it possible to prepare the target products in yields from 13 to 93%.

~70%

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