Journal of combinatorial chemistry

Dynamic Covalent Chemistry of Disulfides Offers a Highly Efficient Synthesis of Diverse Benzofused Nitrogen− Sulfur Heterocycles in One Pot

N Zhu, F Zhang, G Liu

Index: Jacobsen, Niels; Kolind-Andersen, Hans Synthesis, 1990 , # 10 p. 911 - 914

Full Text: HTML

Citation Number: 22

Abstract

... new methods using more stable and simply prepared disulfides to synthesize sulfides or ... in a Tandem Process. Table 5. Detailed Nitrogen−Sulfur Heterocycles Synthesized by This ... figure Scheme 4. Highly Efficient Synthesis of Benzofused Nitrogen−Sulfur Heterocycles in a ...

 Related Synthetic Route
Diethyl malonate Structure

105-53-3

Diethyl malonate

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~81%

(2h)1,4-benzothiazin-3(4h)-one Structure

5325-20-2

(2h)1,4-benzoth...

2-(ethylthio)aniline Structure

13920-91-7

2-(ethylthio)aniline

Methyl 2-phenylacetate Structure

101-41-7

Methyl 2-phenyl...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~85%

9-phenyl-10-thia-7-azabicyclo[4.4.0]deca-1,3,5-trien-8-one Structure

38533-19-6

9-phenyl-10-thi...

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

Methyl cyanoacetate Structure

105-34-0

Methyl cyanoacetate

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~%

2-(2-aminophenyl)sulfanylacetonitrile Structure

62225-57-4

2-(2-aminopheny...

2-methylthioaniline Structure

2987-53-3

2-methylthioaniline

Methyl (2-chlorophenyl)acetate Structure

57486-68-7

Methyl (2-chlor...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~79%

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

9-(2-chlorophenyl)-10-thia-7-azabicyclo[4.4.0]deca-1,3,5-trien-8-one Structure

58553-47-2

9-(2-chlorophen...

Methyl (4-methoxyphenyl)acetate Structure

23786-14-3

Methyl (4-metho...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

2-(4-METHOXYPHENYL)-2H-BENZO[B][1,4]THIAZIN-3(4H)-ONE Structure

92552-87-9

2-(4-METHOXYPHE...

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

Ethyl 4-fluorophenylacetate Structure

587-88-2

Ethyl 4-fluorop...

~0%

2-(4-fluorophenyl)-3-oxo-3,4-dihydro-2H-1,4-benzothiazine Structure

100638-27-5

2-(4-fluorophen...

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

Methyl 4-chlorophenylacetate Structure

52449-43-1

Methyl 4-chloro...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

2-(4-CHLOROPHENYL)-2H-BENZO[B][1,4]THIAZIN-3(4H)-ONE Structure

4652-24-8

2-(4-CHLOROPHEN...

Methyl 1-Naphthaleneacetate Structure

2876-78-0

Methyl 1-Naphth...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

2-(naphthalen-1-yl)-2H-benzo[b][1,4]thiazin-3(4H)-one Structure

131602-98-7

2-(naphthalen-1...

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

Ethyl (4-methylphenyl)acetate Structure

14062-19-2

Ethyl (4-methyl...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

N/A Structure

131602-92-1

N/A

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

(3-bromo-4-methoxy-phenyl)-acetic acid methyl ester Structure

19626-36-9

(3-bromo-4-meth...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

2-(3-bromo-4-methoxyphenyl)-2H-benzo[b][1,4]thiazin-3(4H)-one Structure

131602-96-5

2-(3-bromo-4-me...

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

Methyl (2-chlorophenyl)acetate Structure

57486-68-7

Methyl (2-chlor...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

9-(2-chlorophenyl)-10-thia-7-azabicyclo[4.4.0]deca-1,3,5-trien-8-one Structure

58553-47-2

9-(2-chlorophen...

Ethyl 2-Pyridylacetate Structure

2739-98-2

Ethyl 2-Pyridyl...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

N/A Structure

131602-99-8

N/A

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

Ethyl 2-(pyridin-3-yl)acetate Structure

39931-77-6

Ethyl 2-(pyridi...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

N/A Structure

131603-00-4

N/A

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

1,3-Benzodioxole-5-aceticacid, methyl ester Structure

326-59-0

1,3-Benzodioxol...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

2-(benzo[d][1,3]dioxol-5-yl)-2H-benzo[b][1,4]thiazin-3(4H)-one Structure

131602-97-6

2-(benzo[d][1,3...

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

4-(1-METHYLETHYL)-BENZENEACETIC ACID METHYL ESTER Structure

16216-94-7

4-(1-METHYLETHY...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

2-(4-isopropylphenyl)-2H-benzo[b][1,4]thiazin-3(4H)-one Structure

131602-93-2

2-(4-isopropylp...

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

Methyl [3-(trifluoromethyl)phenyl]acetate Structure

62451-84-7

Methyl [3-(trif...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

N/A Structure

131602-94-3

N/A

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

Ethyl 2-(3,4-dimethoxyphenyl)acetate Structure

18066-68-7

Ethyl 2-(3,4-di...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

Structure

117838-86-5

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol

Methyl 2-phenylacetate Structure

101-41-7

Methyl 2-phenyl...

2,2'-Disulfanediyldianiline Structure

1141-88-4

2,2'-Disulfaned...

~0%

9-phenyl-10-thia-7-azabicyclo[4.4.0]deca-1,3,5-trien-8-one Structure

38533-19-6

9-phenyl-10-thi...

2-Aminothiophenol Structure

137-07-5

2-Aminothiophenol


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