Journal of the American Chemical Society

Justus Liebig's Annalen der Chemie.

GA Prochazka

Index: Chemische Berichte, , vol. 73, p. 450 Justus Liebigs Annalen der Chemie, , vol. 499, p. 1,19 Journal of the Chemical Society, , p. 2607,2610 Canadian Journal of Research, Section B: Chemical Sciences, , vol. 26, p. 783,789 Synthetic Communications, , vol. 36, # 20 p. 3061 - 3064

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Abstract

Methods for the preparation of the mononitrosalicylic acids.(1) 50 grns of nitric acid (1.5 sp. gr.) are added in small portions to a cold solation of 100 gms salicylic acid in 500 or 800 gins glacial acetic acid. The resulting liquid i 4 diluted with 2 or: j vol. water and cooled down very low.(2) 10 gms salicylic acid are gradually added to a mixture of 10 gms fuming nitric and 10 or 12 gnis glacial acetic. acid; the resulting liquid is poured in 250 cc very cold water. The ...