N-Acyl DBN Tetraphenylborate Salts as N-Acylating Agents

JE Taylor, MD Jones, JMJ Williams…

Index: Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin Synthesis, 2002 , # 6 p. 733 - 738

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Citation Number: 15

Abstract

... we investigated whether other stable N-acyl DBN·BPh 4 salts (3b–f) could be synthesized in a ... Table 1. Synthesis of N-Acyl DBN·BPh 4 Salts (3a–f) from DBN (1) and Acyl Chlorides (2a ... DBN·BPh 4 (3b) to give 76% of the corresponding amide (5f) (Table 2, entry 6). Reaction with ...

 Related Synthetic Route
4,5-Dichloro-3(2H)-pyridazinone Structure

932-22-9

4,5-Dichloro-3(...

Propanoyl chloride Structure

79-03-8

Propanoyl chloride

~99%

4,5-Dichloro-2-(1-oxopropyl)-3(2H)-pyridazinone Structure

155164-64-0

4,5-Dichloro-2-...

4,5-Dichloro-3(2H)-pyridazinone Structure

932-22-9

4,5-Dichloro-3(...

Acetyl chloride Structure

75-36-5

Acetyl chloride

~98%

2-acetyl-4,5-dichloropyridazin-3-one Structure

155164-63-9

2-acetyl-4,5-di...

4,5-Dichloro-3(2H)-pyridazinone Structure

932-22-9

4,5-Dichloro-3(...

p-Anisoyl chloride Structure

100-07-2

p-Anisoyl chloride

~85%

4,5-dichloro-2-(4-methoxybenzoyl)pyridazin-3-one Structure

155164-68-4

4,5-dichloro-2-...

Glycine Structure

56-40-6

Glycine

2-benzoyl-4,5-dichloro-pyridazin-3-one Structure

155164-66-2

2-benzoyl-4,5-d...

~95%

Hippuric acid Structure

495-69-2

Hippuric acid

4,5-Dichloro-3(2H)-pyridazinone Structure

932-22-9

4,5-Dichloro-3(...

4-Chlorobenzoyl chloride Structure

122-01-0

4-Chlorobenzoyl...

~80%

4,5-dichloro-2-(4-chlorobenzoyl)pyridazin-3-one Structure

450408-66-9

4,5-dichloro-2-...

Structure

74497-02-2

2-acetyl-4,5-dichloropyridazin-3-one Structure

155164-63-9

2-acetyl-4,5-di...

~92%

Acetanilide Structure

103-84-4

Acetanilide

4-Aminophenol Structure

123-30-8

4-Aminophenol

2-benzoyl-4,5-dichloro-pyridazin-3-one Structure

155164-66-2

2-benzoyl-4,5-d...

~91%

4-(Benzoylamino)phenol Structure

15457-50-8

4-(Benzoylamino...

2-acetyl-4,5-dichloropyridazin-3-one Structure

155164-63-9

2-acetyl-4,5-di...

4-Methylbenzylamine Structure

104-84-7

4-Methylbenzylamine

~99%

ACETAMIDE, N-[(4-METHYLPHENYL)METHYL]- Structure

25079-96-3

ACETAMIDE, N-[(...

Anthranilic acid Structure

118-92-3

Anthranilic acid

2-benzoyl-4,5-dichloro-pyridazin-3-one Structure

155164-66-2

2-benzoyl-4,5-d...

~82%

2-(Benzoylamino)benzoic acid Structure

579-93-1

2-(Benzoylamino...

2-(2-Aminophenyl)ethanol Structure

5339-85-5

2-(2-Aminopheny...

2-acetyl-4,5-dichloropyridazin-3-one Structure

155164-63-9

2-acetyl-4,5-di...

~96%

2-ACETAMIDOPHENETHYL ALCOHOL Structure

69258-86-2

2-ACETAMIDOPHEN...

4,5-Dichloro-3(2H)-pyridazinone Structure

932-22-9

4,5-Dichloro-3(...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~79%

2-benzoyl-4,5-dichloro-pyridazin-3-one Structure

155164-66-2

2-benzoyl-4,5-d...

4,5-Dichloro-3(2H)-pyridazinone Structure

932-22-9

4,5-Dichloro-3(...

p-toluoyl chloride Structure

874-60-2

p-toluoyl chloride

~82%

4,5-dichloro-2-(4-methylbenzoyl)pyridazin-3-one Structure

155164-67-3

4,5-dichloro-2-...

2-benzoyl-4,5-dichloro-pyridazin-3-one Structure

155164-66-2

2-benzoyl-4,5-d...

4-Methylbenzylamine Structure

104-84-7

4-Methylbenzylamine

~95%

N-[(4-methylphenyl)methyl]benzamide Structure

65608-94-8

N-[(4-methylphe...

Benzoyl chloride Structure

98-88-4

Benzoyl chloride

~%

N-[(4-methylphenyl)methyl]benzamide Structure

65608-94-8

N-[(4-methylphe...


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