Tetrahedron letters

Novel trichloroacetyl based silylations: simple methods for t-butyldimethylsilylations and for the protection of amino groups.

AA Galan, TV Lee, CB Chapleo

Index: Galan, Adam A.; Lee, Thomas V.; Chapleo, Christopher B. Tetrahedron Letters, 1986 , vol. 27, # 41 p. 4995 - 4998

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Citation Number: 6

Abstract

... School of Chemistry, The University, Bristol, BS8 1TS, UK. Christopher B Chapleo. (Dept. of Medicinal Chemistry, Reckitt & Colman Ltd., Hull, UK. Received 2 July 1986, Available online 6 April 2001. Abstract. A new reagent for t-butyldimethylsilylation has been developed and the known trimethylsilyl trichloroacetate (1) has been shown to be of use for N-silylating amines. ... References. 1; JM Renga, PC. Wang; Tetrahedron letters, 26 (1985), p. 1175. ...