Glycosyl 1, 2, 3-triazoles with α-d-gluco, β-d-gluco, α-d-galacto, β-d-galacto and β-2- acetamido-2-deoxygluco (GlcNAc) stereochemistry were prepared by reaction of the corresponding azides with vinyl acetate under microwave irradiation. The deprotected glucosyl and galactosyl triazoles did not display inhibitory activity against the tested glycosidases at 1mM. Of the four fungal glycosidases evaluated, GlcNAc-triazole was ...