Direct determination of MCPD fatty acid esters and glycidyl fatty acid esters in vegetable oils by LC–TOFMS

…, RM Pierceall, I Lee, P Venkitasubramanian…

Index: Haines, Troy D.; Adlaf, Kevin J.; Pierceall, Robert M.; Lee, Inmok; Venkitasubramanian, Padmesh; Collison, Mark W. JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 1 p. 1 - 14

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Citation Number: 76

Abstract

Abstract Analysis of MCPD esters and glycidyl esters in vegetable oils using the indirect method proposed by the DGF gave inconsistent results when salting out conditions were varied. Subsequent investigation showed that the method was destroying and reforming MCPD during the analysis. An LC time of flight MS method was developed for direct analysis of both MCPD esters and glycidyl esters in vegetable oils. The results of the LC–TOFMS ...