The Journal of Organic Chemistry

The Chemistry of Sulfur Tetrafluoride. IX. Reaction with Amino Acids in Hydrogen Fluoride1

MS Raasch

Index: Raasch,M.S. Journal of Organic Chemistry, 1962 , vol. 27, p. 1406 - 1409

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Citation Number: 64

Abstract

24. 4, 5-Bis (trifluoromethyl) imidaeole a pH at half-neutralization in ca. 0.02 M solution in HzO, glass electrode. Value for NH, 9.2; n-butylamine, 10.6. b Best result. Difficulty has been encountered in repeating this experiment. The amine was purified by gas chromatography over Dow Corning silicone oil No. 703 on firebrick.