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e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521

Tetrahedron Letters

A selective, tin-free radical mediated synthesis of indoles based on a sulfonate template

VJ Gray, JD Wilden

Index: Tetrahedron Letters, , vol. 53, # 1 p. 41 - 44

Full Text: HTML

Citation Number: 1

Abstract

... Authors: Vincent James Gray; Jonathan D. Wilden. Journal Tetrahedron Letters 0040-4039 Publisher Elsevier Publication Date Jan 01, 2012 Volume 53 Issue 1 Identifiers DOI: 10.1016/j.tetlet.2011.10.093 Keywords: Sulfonate Ester; Indole; Radical; Cyclisation. Abstract. ...

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2,4,6-trichlorophenyl 1-bromo-2-((3-methoxyphenyl)(methyl)amino)ethanesulfonate Structure

1352622-07-1

2,4,6-trichloro...

~28%

6-methoxy-1-methylindole Structure

1968-17-8

6-methoxy-1-met...

4-METHOXY-1-METHYL-1H-INDOLE Structure

7556-35-6

4-METHOXY-1-MET...

N/A Structure

1352622-16-2

N/A

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1-bromo-2-(3-methoxyphenylamino)ethanesulfonic acid 2,4,6-trichlorophenyl ester Structure

1352621-99-8

1-bromo-2-(3-me...

~%

6-methoxy-1-methylindole Structure

1968-17-8

6-methoxy-1-met...

4-METHOXY-1-METHYL-1H-INDOLE Structure

7556-35-6

4-METHOXY-1-MET...

N/A Structure

1352622-16-2

N/A

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Methyl 4-aminobenzoate Structure

619-45-4

Methyl 4-aminob...

~%

N/A Structure

1352622-18-4

N/A

methyl 1-methylindole-5-carboxylate Structure

128742-76-7

methyl 1-methyl...

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2,4,6-trichlorophenyl 1-bromoethenesulfonate Structure

1352621-86-3

2,4,6-trichloro...

methyl 4-methylaminobenzoate Structure

18358-63-9

methyl 4-methyl...

~%

N/A Structure

1352622-18-4

N/A

methyl 1-methylindole-5-carboxylate Structure

128742-76-7

methyl 1-methyl...

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methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate Structure

1352622-01-5

methyl 4-((2-br...

~45%

N/A Structure

1352622-18-4

N/A

methyl 1-methylindole-5-carboxylate Structure

128742-76-7

methyl 1-methyl...

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1-bromo-2-[(4-bromophenyl)methylamino]ethanesulfonic acid 2,4,6-trichlorophenyl ester Structure

1352622-04-8

1-bromo-2-[(4-b...

~39%

5-Bromo-1-methyl-1H-indole Structure

10075-52-2

5-Bromo-1-methy...

N/A Structure

1352622-13-9

N/A

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1-bromo-2-(4-bromophenylamino)ethanesulfonic acid 2,4,6-trichlorophenyl ester Structure

1352621-93-2

1-bromo-2-(4-br...

~%

5-Bromo-1-methyl-1H-indole Structure

10075-52-2

5-Bromo-1-methy...

N/A Structure

1352622-13-9

N/A

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2,4,6-trichlorophenyl 1-bromo-2-(methyl(phenyl)amino)ethanesulfonate Structure

1352621-88-5

2,4,6-trichloro...

~65%

1-Methylindole Structure

603-76-9

1-Methylindole

N/A Structure

1352622-10-6

N/A

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[Kong, Aidi; Han, Xiuling; Lu, Xiyan Organic Letters, 2006 , vol. 8, # 7 p. 1339 - 1342]

Detail Synthetic Route


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