Synthesis of polynitro compounds. Peroxydisulfuric acid oxidation of polynitroarylamines to polynitro aromatics

…, WP Norris, CL Coon, ME Sitzmann

Index: Nielsen, Arnold T.; Atkins, Ronald L.; Norris, William P.; Coon, Clifford L.; Sitzmann, Michael E. Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2341 - 2347

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Citation Number: 30

Abstract

Peroxydisulfuric acid in sulfuric acid solution, prepared by reaction of hydrogen peroxide with excess oleum or 100% H2S04, oxidizes primary polynitroarylamines and their N- acetamido derivatives to polynitro aromatics in good to excellent yields. The new ...