Flexidentate Behaviour of 2??Pyridylsulfonamides− Direct Electrochemical Synthesis and Spectroscopic and X??ray Characterisation of Neutral Copper (II) Complexes …

…, JA García??Vázquez, P Pérez??Lourido…

Index: Beloso, Inmaculada; Borras, Joaquin; Castro, Jesus; Garcia-Vazquez, Jose A.; Perez-Lourido, Paulo; Romero, Jaime; Sousa, Antonio European Journal of Inorganic Chemistry, 2004 , # 3 p. 635 - 645

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Citation Number: 15

Abstract

Abstract Copper complexes with potentially bidentate N-(2-pyridyl) sulfonylamide ligands have been synthesised by the electrochemical oxidation of the metal in an acetonitrile solution of the neutral amide and additional bidentate N− N coligands. The compounds have been characterised by microanalysis and EPR, vibrational and electronic spectroscopy. In representative cases the structures were also determined by X-ray diffraction methods. ...