Synthesis by the Amine-Hydroperoxide Adduct Method.-The amine-hydroperoxide adduct synthesis of silyl peroxides requires two steps:(1) preparation of the amine-hydroperoxide adduct;(2) reaction of the adduct with chlorosilane in an inert solvent. Preparation of the adduct is carried out by mixing stoichiometric amounts of a suitable amine and the hydroperoxide in an inert solvent. 6 Assuming that the proper sol-vent has been selected, ...
