e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521
Tetrahedron letters
Mannich reactions of π-excessive heterocycles using bis-(dialkylamino) methanes and alkoxydialkylaminomethanes activated with acetyl chloride or sulphur dioxide
SC Eyley, H Heaney, G Papageorgiou, RF Wilkins
Index: Eyley, Stephen C.; Heaney, Harry; Papageorgiou, George; Wilkins, Robert F. Tetrahedron Letters, 1988 , vol. 29, # 24 p. 2997 - 3000
Abstract Π-Excessive heterocycles react rapidly with bis (dialkylamino) methanes (aminals) and alkoxydialkylaminomethanes (aminol ethers) in acetonitrile to afford Mannich bases in good yields when activated by means of an acidic reagent such as acetyl chloride or sulphur dioxide: the principal compound studied was Full-size image (< 1 K)