Microwave-Assisted Synthesis of Disulfides

H Kutuk, N Turkoz

Index: Kutuk, Halil; Turkoz, Nalan Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 7 p. 1515 - 1522

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Citation Number: 2

Abstract

Abstract A new microwave-assisted synthesis methodology for the preparation of substituted disulfide derivatives is presented. 4-Substituted sulfenimides were reacted with 4-substituted thiols under neat (to right doughy consistency) conditions in chloroform, with both microwave heating and conventional methods. The resulting 4-substituted disulfide derivatives were obtained at higher yields and in shorter reaction times with microwave heating. Their ...