Selective deprotection of trialkylsilyl ethers using fluorosilicic acid

…, DK Hill, SJ Shimshock, RE Waltermire…

Index: Pilcher, Anthony S.; Hill, David K.; Shimshock, Stephen J.; Waltermire, Robert E.; DeShong, Philip Journal of Organic Chemistry, 1992 , vol. 57, # 8 p. 2492 - 2495

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Citation Number: 70

Abstract

Conclusions In conclusion, we have described a general, new and simple procedure for the synthesis of 3'-carbonates of pyrimidine and purine 2'-deoxynucleosides. In this me-thod, no previous protection of the primary hydroxyl group is necessary, as has been traditionally described for preparation of these compounds.