The Journal of Organic Chemistry

Improved protocols for the selective deprotection of trialkylsilyl ethers using fluorosilicic acid

AS Pilcher, P DeShong

Index: Pilcher, Anthony S.; DeShong, Philip Journal of Organic Chemistry, 1993 , vol. 58, # 19 p. 5130 - 5134

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Citation Number: 60

Abstract

Improvements for the application of aqueous fluorosilicic acid to the selective cleavage of tertbutyldimethylsilyl ethers in the presence of triisopropylsilyl ethers are described. Deprotection conditions have been optimized for cleavage selectivity, tolerance by acid- ...