Preparation and palladium-catalysed arylation of indolylzinc halides

…, Y Kondo, N Takazawa, H Yamanaka

Index: Sakamoto, Takao; Kondo, Yoshinori; Takazawa, Nobuo; Yamanaka, Hiroshi Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 16 p. 1927 - 1934

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Citation Number: 35

Abstract

Faculty of Pharmaceutical Sciences, Tohoku University Aobayama, Aoba-ku, Sendai 980- 77, Japan ... Indolylzinc halides are prepared by two methods: transmetallation of indolyllithiums with zinc chloride and oxidative addition of active zinc to iodoindoles. The palladium-catalysed reaction of the indolylzinc halides provides a practical method for synthesizing arylindoles. ... Organozinc derivatives have importance in synthetic organic chemistry because of their ...

 Related Synthetic Route
Indole Structure

120-72-9

Indole

~%

1-(benzenesulfonyl)-2-phenylindole Structure

114650-12-3

1-(benzenesulfo...

1-(Phenylsulfonyl)-1H-indole Structure

40899-71-6

1-(Phenylsulfon...

Iodobenzene Structure

591-50-4

Iodobenzene

~%

1-(benzenesulfonyl)-2-phenylindole Structure

114650-12-3

1-(benzenesulfo...

Indole Structure

120-72-9

Indole

~%

3-PHENYL-1-(PHENYLSULFONYL)INDOLE Structure

153827-73-7

3-PHENYL-1-(PHE...

3-Iodoindole Structure

26340-47-6

3-Iodoindole

~%

3-PHENYL-1-(PHENYLSULFONYL)INDOLE Structure

153827-73-7

3-PHENYL-1-(PHE...

Indole Structure

120-72-9

Indole

~%

2-(Thiophen-2-yl)-1H-indole Structure

55968-16-6

2-(Thiophen-2-y...

Methanol Structure

67-56-1

Methanol

carbon monoxide Structure

201230-82-2

carbon monoxide

3-Iodo-1-(phenylsulfonyl)-1H-indole Structure

80360-14-1

3-Iodo-1-(pheny...

~72%

METHYL 1-(PHENYLSULFONYL)-1H-INDOLE-3-CARBOXYLATE Structure

116325-17-8

METHYL 1-(PHENY...

Indole Structure

120-72-9

Indole

~%

METHYL 1-(PHENYLSULFONYL)-1H-INDOLE-3-CARBOXYLATE Structure

116325-17-8

METHYL 1-(PHENY...

3-Iodoindole Structure

26340-47-6

3-Iodoindole

~%

METHYL 1-(PHENYLSULFONYL)-1H-INDOLE-3-CARBOXYLATE Structure

116325-17-8

METHYL 1-(PHENY...

2-Bromo-6-methylpyridine Structure

5315-25-3

2-Bromo-6-methy...

~%

6-bromo-N,N-dimethylpyridine-2-carboxamide Structure

153435-70-2

6-bromo-N,N-dim...

6-Bromopicolinic acid Structure

21190-87-4

6-Bromopicolini...

~%

6-bromo-N,N-dimethylpyridine-2-carboxamide Structure

153435-70-2

6-bromo-N,N-dim...

6-bromopicolinic acid chloride Structure

139487-69-7

6-bromopicolini...

Dimethylamine Structure

124-40-3

Dimethylamine

~%

6-bromo-N,N-dimethylpyridine-2-carboxamide Structure

153435-70-2

6-bromo-N,N-dim...


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