Tetrahedron

N, N′-Linked 1, 2-ethanediyl-poly (benzimidazolin-2-ones) and the X-ray crystal structure of a benzimidazolin-2-one trimer

E Díez-Barra, J Dotor, A de la Hoz, C Foces-Foces…

Index: Diez-Barra, Enrique; Dotor, Julio; De La Hoz, Antonio; Foces-Foces, Concepcion; Enjalbal, Christine; Aubagnac, Jean Louis; Claramunt, Rosa Maria; Elguero, Jose Tetrahedron, 1997 , vol. 53, # 22 p. 7689 - 7704

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Citation Number: 4

Abstract

A series of N, N′-linked 1, 2-ethanediyl-poly (benzimidazolin-2-ones) that can be classified as podands, are described. Seven dimers (21–27), three trimers (28–30), a cyclic tetramer (31) and an open-chain benzimidazolin-2-one heptamer (32) have been prepared and characterized by 1H, 13C NMR and by MS. The crystal and molecular structure of the trimer, 1, 3-bis-2-(2-oxobenzimidazol-1-yl) ethyl-2-oxobenzimidazole monohydrate (30) has ...