Stereocontrolled Total Synthesis of (+)-Paraherquamide B⊥

TD Cushing, JF Sanz-Cervera…

Index: Campbell, John B. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1213 - 1218

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Citation Number: 136

Abstract

... Journal of the ... J. Am ... a Reagents and conditions: (a) 36, 0.5 equiv of PBu 3 , MeCN, 51%; (b) DMAP, Et 3 N, BOC 2 O, CH 2 Cl 2 , 90%; (c) 5 equiv of LiCl, 1.5 equiv of H 2 O, HMPA, 100 °C, 66%; (d) 3.0 equiv of n-Bu 4 NF, THF, 79%; (e) 1.9 equiv of LiCl, 4.0 equiv of collidine, 4.0 ...