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C.I.颜料黄14

C.I.颜料黄14用途

颜料黄14是一种荧光染料[1]。

C.I.颜料黄14名称

[ CAS 号 ]:
5468-75-7

[ 中文名 ]:
C.I.颜料黄14

[ 英文名 ]:
Pigment Yellow 14

[中文别名 ]:

[英文别名 ]:

Resorcin Brown R
Lake Yellow GA
Benzidine Yellow L
Light Yellow JBV
Plastol Yellow GP
Plastol Yellow GG
Pigment Yellow 14
Pigment Fast Yellow GP
Benzidene Yellow G
Radiant Yellow

C.I.颜料黄14生物活性

[ 描述 ]:

颜料黄14是一种荧光染料[1]。

[ 相关类别 ]:

研究领域 >> 其他

[参考文献]

[1]. Fa-Jun Wang, et al. Continuous-Flow Synthesis of the Azo Pigment Yellow 14 Using a Three-Stream Micromixing Process. Org. Process Res. Dev. 2019, 23, 12, 2637-2646.

C.I.颜料黄14物理化学性质

[ 密度 ]:
1.32 g/cm3

[ 沸点 ]:
793.4ºC at 760 mmHg

[ 分子式 ]:
C₃₄H₃₀Cl₂N₆O₄

[ 分子量 ]:
657.55

[ 闪点 ]:
433.6ºC

[ 精确质量 ]:
656.17100

[ PSA ]:
141.78000

[ LogP ]:
8.78320

[ 外观性状 ]:
黄色粉末带有红色

[ 折射率 ]:
1.64

C.I.颜料黄14毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: EJ3512500

CHEMICAL NAME :: Butanamide, 2,2'-((3,3'-dichloro(1,1'-biphenyl)-4,4'-diyl)bis(azo ))bis(N-(2-methylphen yl)-3- oxo-

CAS REGISTRY NUMBER :: 5468-75-7

LAST UPDATED :: 199710

DATA ITEMS CITED :: 6

MOLECULAR FORMULA :: C34-H30-Cl2-N6-O4

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Oral

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: >5 gm/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: EPASR* United States Environmental Protection Agency, Office of Pesticides and Toxic Substances. (U.S. Environmental Protection Agency, 401 M St., SW, Washington, DC 20460) History unknown. Volume(issue)/page/year: 8EHQ-0690-0962 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOHS - National Occupational Hazard Survey (1974) NOHS Hazard Code - M2152 No. of Facilities: 1317 (estimated) No. of Industries: 23 No. of Occupations: 38 No. of Employees: 25076 (estimated) NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - M2152 No. of Facilities: 4145 (estimated) No. of Industries: 45 No. of Occupations: 46 No. of Employees: 76941 (estimated) No. of Female Employees: 11668 (estimated)

C.I.颜料黄14安全信息

[ 风险声明 (欧洲) ]:
R36/37/38

[ 安全声明 (欧洲) ]:
S26-S37-S39

[ RTECS号 ]:
EJ3512500

C.I.颜料黄14制备

方法1:由3，3'-二氯联苯胺重氮化后，与乙酰乙酰苯胺进行偶合，而后经过滤、干燥等处理过程而制产品。1.重氮化2.偶合产品要求色光与标准品近似，着色力为标准品100±5（分），水分含量≤2%，吸油量50±5%，水溶性盐含量≤1.5%，耐热性180℃，耐晒性5-6级，耐酸性、耐碱性均为1-2级，水渗性、油渗性均为1-2级，乙醇渗性1级，石蜡渗性2级，细度（通过60筛余物含量）≤5%。原料消耗（kg/t）3，3'-二氯联苯胺（100%） 410乙酰乙酰苯胺（100%） 590盐酸（31%） 930亚硝酸钠（工业） 235纯碱（工业） 495冰醋酸 615活性炭 10太古油 55方法2:由邻硝基氯苯出发，在烧碱溶液介质中用锌粉还原，并缩合为2，2'- 二氯二苯肼。再用盐酸处理。转位成3，3'二氯联苯胺盐酸盐。而后将3，3'-二氯联苯胺重氮化，再与邻-乙酰乙酰甲苯胺进行偶合，而得到产品。1.还原缩合2.转位、盐析3.重氮化、偶合