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右旋樟脑磺酸

右旋樟脑磺酸用途

【用途一】
用于医药中间体或异构体产品拆分
【用途二】
用于制药工业
【用途三】
有机合成中间体，拆分剂。

右旋樟脑磺酸名称

[ CAS 号 ]:
3144-16-9

[ 中文名 ]:
D(+)-10-樟脑磺酸

[ 英文名 ]:
D-Camphorsulfonic acid

[中文别名 ]:

[英文别名 ]:

10-Bornanesulfonic acid, 2-oxo-, (1S,4R)-(+)-
b-Camphorsulfonic Acid
UNII:D8D049375Q
D-CAMPHORSULFONIC ACID
(1S)-Camphor-10-sulfonic acid
D-(+)-10-Camphorsulfonic Acid
(+)-Camphor-w-sulfonic Acid
(+)-D-Camphor-10-sulfonic Acid
CSA
camphersulfosaeure

右旋樟脑磺酸物理化学性质

[ 密度 ]:
1.3±0.1 g/cm3

[ 熔点 ]:
195ºC

[ 分子式 ]:
C₁₀H₁₆O₄S

[ 分子量 ]:
232.297

[ 精确质量 ]:
232.076935

[ PSA ]:
79.82000

[ LogP ]:
-0.57

[ 外观性状 ]:
白色结晶粉末

[ 折射率 ]:
1.540

[ 储存条件 ]:
存放于惰性气体之中;避免湿气 (吸湿)

[ 水溶解性 ]:
水溶性：可溶；不溶：乙醚

右旋樟脑磺酸MSDS

右旋樟脑磺酸毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: ED1550000

CHEMICAL NAME :: 10-Bornanesulfonic acid, 2-oxo-, (1S,4R)-(+)-

CAS REGISTRY NUMBER :: 3144-16-9

LAST UPDATED :: 199701

DATA ITEMS CITED :: 2

MOLECULAR FORMULA :: C10-H16-O4-S

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Subcutaneous

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 2502 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: PHARAT Pharmazie. (VEB Verlag Volk und Gesundheit, Neue Gruenstr. 18, Berlin DDR-1020, Ger. Dem. Rep.) V.1- 1946- Volume(issue)/page/year: 1,150,1946

右旋樟脑磺酸安全信息

[ 符号 ]:

GHS05

[ 信号词 ]:
Danger

[ 危害声明 ]:
H314

[ 警示性声明 ]:
P260-P280-P303 + P361 + P353-P304 + P340 + P310-P305 + P351 + P338

[ 个人防护装备 ]:
Eyeshields;Faceshields;full-face particle respirator type N100 (US);Gloves;respirator cartridge type N100 (US);type P1 (EN143) respirator filter;type P3 (EN 143) respirator cartridges

[ 危害码 (欧洲) ]:
C:Corrosive

[ 风险声明 (欧洲) ]:
R34

[ 安全声明 (欧洲) ]:
S25-S36/37/39-S45

[ 危险品运输编码 ]:
UN 3261 8/PG 2

[ WGK德国 ]:
3

[ RTECS号 ]:
ED1550000

[ 包装等级 ]:
III

[ 危险类别 ]:
8.0

[ 海关编码 ]:
29147090

右旋樟脑磺酸合成路线

右旋樟脑磺酸上下游产品

右旋樟脑磺酸上游产品

右旋樟脑磺酸下游产品

右旋樟脑磺酸制备

通过樟脑与乙酸-硫酸酐发生磺化作用，并用乙酸乙酯重结晶纯化制备。

右旋樟脑磺酸海关

[ 海关编码 ]: 2914299000

[ 中文概述 ]:
2914299000. 其他不含其他含氧基的环烷酮、环烯酮或环萜烯酮. 增值税率:17.0%. 退税率:13.0%. 监管条件:无. 最惠国关税:5.5%. 普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途, 丙酮报明包装

[ Summary ]:
2914299000. other cyclanic, cyclenic or cyclotherpenic ketones without other oxygen function. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:5.5%. General tariff:30.0%

右旋樟脑磺酸文献

Salt Stability - The Effect of pHmax on Salt to Free Base Conversion.

Pharm. Res. 32 , 3110-8, (2015)

The aim of this study was to investigate how the disproportionation process can be impacted by the properties of the salt, specifically pHmax.Five miconazole salts and four sertraline salts were selec...

Analysis of deprotonated acids with silicon nanoparticle-assisted laser desorption/ ionization mass spectrometry.

J. Mass Spectrom. 45(12) , 1394-401, (2010)

Chemically modified silicon nanoparticles were applied for the laser desorption/negative ionization of small acids. A series of substituted sulfonic acids and fatty acids was studied. Compared to deso...

Camphorsulfonic acid catalysed facile tandem double Friedlander annulation protocol for the synthesis of phenoxy linked bisquinoline derivatives and discovery of antitubercular agents.

Bioorg. Med. Chem. Lett. 22 , 1643-8, (2012)

A series of phenoxy linked bisquinoline derivatives were synthesised from the Friedlander annulation of 2-(4-acetylphenoxy)-1-aryl-1-ethanones with 2-aminobenzophenone in good yields using (±)-camphor...

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