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1,2,2,3-四氯丙烷

1,2,2,3-四氯丙烷用途

【用途一】
四氯丙烷是除草剂燕麦敌的中间体。

1,2,2,3-四氯丙烷名称

[ CAS 号 ]:
13116-53-5

[ 中文名 ]:
四氯丙烷

[ 英文名 ]:
1,2,2,3-TETRACHLOROPROPANE

[英文别名 ]:

1,2,2,3-TETRACHLOROPROPANE
MFCD00039362
Propane, 1,2,2,3-tetrachloro-
EINECS 236-043-9

1,2,2,3-四氯丙烷物理化学性质

[ 密度 ]:
1.5±0.1 g/cm3

[ 沸点 ]:
176.3±8.0 °C at 760 mmHg

[ 分子式 ]:
C₃H₄Cl₄

[ 分子量 ]:
181.876

[ 闪点 ]:
62.5±15.8 °C

[ 精确质量 ]:
179.906708

[ LogP ]:
2.46

[ 蒸汽压 ]:
1.5±0.3 mmHg at 25°C

[ 折射率 ]:
1.483

[ 储存条件 ]:
室温

1,2,2,3-四氯丙烷MSDS

详细MSDS(安全技术说明书)

1,2,2,3-四氯丙烷毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: TZ7000100

CHEMICAL NAME :: Propane, 1,2,2,3-tetrachloro-

CAS REGISTRY NUMBER :: 13116-53-5

BEILSTEIN REFERENCE NO. :: 1734971

LAST UPDATED :: 199710

DATA ITEMS CITED :: 7

MOLECULAR FORMULA :: C3-H4-Cl4

MOLECULAR WEIGHT :: 181.87

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Oral

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: 6300 mg/kg

TOXIC EFFECTS :: Behavioral - somnolence (general depressed activity) Behavioral - food intake (animal) Gastrointestinal - other changes

REFERENCE :: NTIS** National Technical Information Service. (Springfield, VA 22161) Formerly U.S. Clearinghouse for Scientific & Technical Information. Volume(issue)/page/year: OTS0570609

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Administration onto the skin

SPECIES OBSERVED :: Rodent - rabbit

DOSE/DURATION :: >7940 mg/kg

TOXIC EFFECTS :: Behavioral - somnolence (general depressed activity) Behavioral - food intake (animal)

REFERENCE :: NTIS** National Technical Information Service. (Springfield, VA 22161) Formerly U.S. Clearinghouse for Scientific & Technical Information. Volume(issue)/page/year: OTS0570609 ** OTHER MULTIPLE DOSE TOXICITY DATA **

TYPE OF TEST :: TCLo - Lowest published toxic concentration

ROUTE OF EXPOSURE :: Inhalation

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: 568 ppm/6H/4W-I

TOXIC EFFECTS :: Sense Organs and Special Senses (Eye) - lacrimation Nutritional and Gross Metabolic - weight loss or decreased weight gain Related to Chronic Data - death

REFERENCE :: JTEHD6 Journal of Toxicology and Environmental Health. (Hemisphere Pub., 1025 Vermont Ave., NW, Washington, DC 20005) V.1- 1975/76- Volume(issue)/page/year: 25,317,1988

TYPE OF TEST :: TCLo - Lowest published toxic concentration

ROUTE OF EXPOSURE :: Inhalation

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: 13 ppm/6H/13W-I

TOXIC EFFECTS :: Liver - changes in liver weight Blood - changes in leukocyte (WBC) count

REFERENCE :: JTEHD6 Journal of Toxicology and Environmental Health. (Hemisphere Pub., 1025 Vermont Ave., NW, Washington, DC 20005) V.1- 1975/76- Volume(issue)/page/year: 25,317,1988 ** REPRODUCTIVE DATA **

TYPE OF TEST :: TCLo - Lowest published toxic concentration

ROUTE OF EXPOSURE :: Inhalation

DOSE :: 15 ppm/6H

SEX/DURATION :: male 10 week(s) pre-mating female 10 week(s) pre-mating - 2 week(s) after conception

TOXIC EFFECTS :: Reproductive - Fertility - mating performance (e.g. # sperm positive females per # females mated; # copulations per # estrus cycles)

REFERENCE :: JTEHD6 Journal of Toxicology and Environmental Health. (Hemisphere Pub., 1025 Vermont Ave., NW, Washington, DC 20005) V.1- 1975/76- Volume(issue)/page/year: 25,317,1988

1,2,2,3-四氯丙烷安全信息

[ RTECS号 ]:
TZ7000100

[ 海关编码 ]:
2903199000

1,2,2,3-四氯丙烷合成路线

详细合成路线

1,2,2,3-四氯丙烷上下游产品

1,2,2,3-四氯丙烷上游产品

1,2,2,3-四氯丙烷下游产品

1,2,2,3-四氯丙烷制备

其制备方法是在反应釜中加入溶剂四氯化碳和2，3-二氯丙烯，于10～15℃通氯气，通入一定量氯气后，水洗，再用Na2CO3溶液洗，再水洗至中性，脱溶，减压蒸馏，收集84～90℃/40～53 kPa馏分即为成品。

ClCH2CCl=CH2+Cl2→ClCH2CCl2CH2Cl

1,2,2,3-四氯丙烷海关

[ 海关编码 ]: 2903199000

[ 中文概述 ]:
2903199000 其他无环烃的饱和氯化衍生物。监管条件:无。增值税率:17.0%。退税率:9.0%。最惠国关税:5.5%。普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途

[ Summary ]:
2903199000 other saturated chlorinated derivatives of acyclic hydrocarbons。Supervision conditions:None。VAT:17.0%。Tax rebate rate:9.0%。MFN tariff:5.5%。General tariff:30.0%