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4-正丁基苯胺

4-正丁基苯胺用途

【用途一】
染料中间体。用于生产卡普蓝、绿GS、5GS等。

4-正丁基苯胺名称

[ CAS 号 ]:
104-13-2

[ 中文名 ]:
4-正丁基苯胺

[ 英文名 ]:
4-Butylaniline

[中文别名 ]:

对正丁基苯胺

[英文别名 ]:

4-Butylaniline
Aniline, 4-butyl-
4-n-BuC6H4NH2
EINECS 203-177-4
p-Aminobutylbenzene
p-n-Butylaniline
4-n-butylbenzenamine
Aniline, p-butyl-
4-butylphenylamine
p-Butylaminobenzene

4-正丁基苯胺物理化学性质

[ 密度 ]:
0.9±0.1 g/cm3

[ 沸点 ]:
261.0±0.0 °C at 760 mmHg

[ 熔点 ]:
-14°C

[ 分子式 ]:
C₁₀H₁₅N

[ 分子量 ]:
149.233

[ 闪点 ]:
101.7±0.0 °C

[ 精确质量 ]:
149.120453

[ PSA ]:
26.02000

[ LogP ]:
2.99

[ 外观性状 ]:
透明无色非固定的液体,带有一种像空气的气味

[ 蒸汽压 ]:
0.0±0.5 mmHg at 25°C

[ 折射率 ]:
1.538

[ 储存条件 ]:
库房通风低温干燥

4-正丁基苯胺MSDS

4-正丁基苯胺毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: BW9470000

CHEMICAL NAME :: Aniline, 4-butyl-

CAS REGISTRY NUMBER :: 104-13-2

BEILSTEIN REFERENCE NO. :: 1447268

LAST UPDATED :: 199710

DATA ITEMS CITED :: 5

MOLECULAR FORMULA :: C10-H15-N

MOLECULAR WEIGHT :: 149.26

WISWESSER LINE NOTATION :: ZR D4

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Intraperitoneal

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 81 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: JMCMAR Journal of Medicinal Chemistry. (American Chemical Soc., Distribution Office Dept. 223, POB POB 57136, West End Stn., Washington, DC 20037) V.6- 1963- Volume(issue)/page/year: 17,900,1974 ** OTHER MULTIPLE DOSE TOXICITY DATA **

TYPE OF TEST :: TDLo - Lowest published toxic dose

ROUTE OF EXPOSURE :: Administration onto the skin

SPECIES OBSERVED :: Rodent - rabbit

DOSE/DURATION :: 3 mL/kg/3D-I

TOXIC EFFECTS :: Liver - hepatitis (hepatocellular necrosis), zonal Kidney, Ureter, Bladder - inflammation, necrosis, or scarring of bladder Related to Chronic Data - death

REFERENCE :: TXAPA9 Toxicology and Applied Pharmacology. (Academic Press, Inc., 1 E. First St., Duluth, MN 55802) V.1- 1959- Volume(issue)/page/year: 12,302,1968

4-正丁基苯胺安全信息

[ 符号 ]:

GHS06

[ 信号词 ]:
Danger

[ 危害声明 ]:
H301 + H311 + H331-H315-H319-H335-H412

[ 警示性声明 ]:
P261-P273-P280-P301 + P310-P305 + P351 + P338-P311

[ 个人防护装备 ]:
Eyeshields;Faceshields;full-face respirator (US);Gloves;multi-purpose combination respirator cartridge (US);type ABEK (EN14387) respirator filter

[ 危害码 (欧洲) ]:
T:Toxic;

[ 风险声明 (欧洲) ]:
R23/24/25;R36/37/38

[ 安全声明 (欧洲) ]:
S23-S26-S36/37/39-S45

[ 危险品运输编码 ]:
UN 2810 6.1/PG 3

[ WGK德国 ]:
3

[ RTECS号 ]:
BW9470000

[ 包装等级 ]:
II

[ 危险类别 ]:
6.1

[ 海关编码 ]:
29214980

4-正丁基苯胺合成路线

4-正丁基苯胺上下游产品

4-正丁基苯胺上游产品

4-正丁基苯胺下游产品

4-正丁基苯胺制备

由苯胺与丁醇在氯化锌存在下反应而得。将1mol苯胺、1mol丁醇、6.5mol无水氯化锌加热到121℃，压力为0.78MPa，反应6h后再升温240℃，压力为2.06-2.16MPa，反应10h至终点。取反应物在碱液中回流5h，分离得粗品4.5-5kg，收率40-45%。

4-正丁基苯胺海关

[ 海关编码 ]: 2921420090

[ 中文概述 ]:
2921420090 其他苯胺衍生物及其盐. 增值税率:17.0% 退税率:9.0% 监管条件:无最惠国关税:6.5% 普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途

[ Summary ]:
HS:2921420090 aniline derivatives and their salts VAT:17.0% Tax rebate rate:9.0% Supervision conditions:none MFN tariff:6.5% General tariff:30.0%

4-正丁基苯胺文献

HEK293S cells have functional retinoid processing machinery.

J. Gen. Physiol. 119(6) , 593-612, (2002)

Rhodopsin activation is measured by the early receptor current (ERC), a conformation-associated charge motion, in human embryonic kidney cells (HEK293S) expressing opsins. After rhodopsin bleaching in...

Mixed-mode reversed-phase and ion-exchange monolithic columns for micro-HPLC.

J. Sep. Sci. 31(15) , 2774-83, (2008)

This paper describes the fabrication of RP/ion-exchange mixed-mode monolithic materials for capillary LC. Following deactivation of the capillary surface with 3-(trimethoxysilyl)propyl methacrylate (g...

Preparation of 4-butylaniline-bonded attapulgite for pre-concentration of bisphenol A in trace quantity.

Talanta 136 , 29-34, (2015)

Ring-opening reaction with synchronous hydrolysis was used to prepare 4-butylaniline-modified attapulgite (abbreviated as BA-ATP) for pre-concentration of bisphenol A (BPA) in trace quantity. The prep...

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