Journal of the American Chemical Society

α-Bromosulfones1

WM Ziegler, R Connor

文献索引：Ziegler; Connor Journal of the American Chemical Society, 1940 , vol. 62, p. 2598

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被引用次数: 29

摘要

2598 WILLIAM M. ZIEGLER AND RALPH CONNOR Vol. 62 weighed 248 g.(92%), mp 177- 179". Recrystallization from alcohol-acetic acid (3: 1) gave pure l, 2-di-n-butylsulfonylethane melting at 180-181'. I7 To 172 g. of the crude disulfone in 360 ml. of 50% alcohol was added 175 g. of potassium cyanide and the mixture refluxed for twenty-four hours. About 185 ml. of solvent was removed by distillation, the residue diluted with 200 ml. of water and 480 ml. ...