The Catalytic Reduction of Dinitroneopentane

J Rockett, FC Whitmore

文献索引：Rockett; Whitmore Journal of the American Chemical Society, 1949 , vol. 71, p. 3250

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被引用次数: 7

摘要

ExDerimental C, 56.35; H, 6.83. 4-Carbomethoxy-4-methylcyclohexene (I11 j.-A mixture of 100 g.(1.0 mole) of methyl methacrylate, 108 g.(2 moles) of butadiene and 1 g. of hydroquinone2 was heated in a steel hydrogenation bomb at 180" for fifteen hours. The viscous product was distilled from a Claisen flask under reduced pressure to separate the polymeric materials and the distillate fractionated through a 2 X 40 cm. glass-helix packed ...